Pb-TKX-50燃烧催化剂的合成及热分解性能

以二氯乙二肟、二甲基甲酰胺、叠氮化钠、盐酸羟胺和硝酸铅等为原料,合成了1,1-二羟基-5,5′-联四唑羟胺铅盐(Pb-TKX-50)燃烧催化剂,研究了Pb-TKX-50对推进剂机械感度的影响以及与推进剂组分的相容性;利用差示扫描量热法和热重法研究了Pb-TKX-50在不同升温速率下的热分解过程,计算其表观活化能(E K和E O)和指前因子(A K),得到其热分解动力学参数、热分解机理函数、热爆炸温度和热力学性质。结果表明,在推进剂配方中加入Pb-TKX-50燃烧催化剂,可以改善其撞击感度和摩擦感度,且与推进剂组分的相容性良好;Pb-TKX-50的主峰分解温度相对于TKX-50的主峰分解温度显著提高,说明其热稳定性显著提高。Ozawa法和Kissinger法得到Pb-TKX-50的表观活化能分别为181.45 kJ/mol和182.49 kJ/mol,且热分解过程符合Avrami-Erofeev方程;Pb-TKX-50的自加速分解温度和爆炸临界温度分别为500.53 K和544.33 K,表明其热稳定性良好;Pb-TKX-50催化剂的热分解自由能(ΔG^≠)为158.87 kJ/mol,活化焓(ΔH^≠)为187.03 kJ/mol,活化熵(ΔS≠)为52.98 kJ/mol。     

面向机电设备评估的重置成本法及应用研究

由于市场的局限性和设备创造价值的不可分割性，重置成本法在机电设备评估实践中得到了广泛应用。但在应用该方法获取评估值时，对于基本公式的选择以及三大贬值或综合成新率的确定目前存在很大分歧。基于重置成本法的基本公式和定义，综合考虑了机器设备的有形损耗和无形磨损，以实体性贬值、功能性贬值和经济性贬值为基础建立了因素集，并建立了科学合理的计算设备价值的方法，对评估价值量较小且单一的机械设备的价格具有一定的实际意义和参考价值。     

Multisensor data fusion via Gaussian process models for dimensional and geometric verification

An increasing amount of commercial measurement instruments implementing a wide range of measurement technologies is rapidly becoming available for dimensional and geometric verification. Multiple solutions are often acquired within the shop-floor with the aim of providing alternatives to cover a wider array of measurement needs, thus overcoming the limitations of individual instruments and technologies.In such scenarios, multisensor data fusion aims at going one step further by seeking original and different ways to analyze and combine multiple measurement datasets taken from the same measurand, in order to produce synergistic effects and ultimately obtain overall better measurement results.In this work an original approach to multisensor data fusion is presented, based on the development of Gaussian process models (the technique also known as kriging), starting from point sets acquired from multiple instruments. The approach is illustrated and validated through the application to a simulated test case and two real-life industrial metrology scenarios involving structured light scanners and coordinate measurement machines.The results show that not only the proposed approach allows for obtaining final measurement results whose metrological quality transcends that of the original single-sensor datasets, but also it allows to better characterize metrological performance and potential sources of measurement error originated from within each individual sensor.     

篮球技术多媒体CAI课件在体育教学中的研究与应用价值分析

随着科学技术水平的不断提高，在学校教育中应用多媒体CAI的现象越来越普遍，并且受到了广大师生的喜爱。在篮球技术教学中，多媒体CAI课件得到了广泛的应用，并且发挥了非常重要的作用，促进了学生篮球技术水平的提高，实现了预期的教学效果。     

直接熔样正热电离质谱法测定二硼化锆中硼同位素丰度

本工作选择m/z88(23 Na210BO2+)和m/z89(23 Na211BO2+)的Na2BO2+作为检测离子,研究了同位素干扰、涂样技术、ZrB2样品处理等对硼同位素测定的影响,建立了快速准确测定ZrB2中硼同位素丰度的正热电离质谱法。实验复现了硼同位素标准物质的标准值,对酸溶法分解试样后涂样和直接熔融法涂样测量结果的精密度进行了比较。结果表明,采用直接熔融法涂样可以快速准确地测定ZrB2中硼同位素丰度,δ10B同位素丰度测定结果精密度优于0.020%。     

Teff (Eragrostis tef) processing,utilization and future opportunities: a review

The demand for food production has been constantly increasing due to rising population. In developed countries, for example, the emergence of regional production of old grains that are rarely utilized, along with the production of commonly consumed grains, has gained importance in recent years. These grains, known collectively as ancient or heirloom grains, have offered both farmers and consumers novel ways of cultivation and products with interesting taste, characteristics and nutritional value. Among the 30 000 plant species known, only five cereals currently provide more than 50% of the world's energy intake – bread wheat (Triticum aestivum), rice (Oryza sativa), sorghum (Sorghum bicolor), millets (Panicum sp.) and maize (Zea mays). The excessive utilization of these selected species has a great potential to cause genetic losses and difficulty in bridging future agricultural demands. Teff (Eragrostis tef), an ancient grain extensively cultivated in countries like Eritrea and Ethiopia, provides promising alternatives for new food uses since its nutritional value is significantly higher than most others cereal grains. The absence of gluten allows flexibility in food utilization since it can be directly substituted to gluten-containing products. The grain also offers an excellent balance of essential amino acids and minerals, which can fulfil the recommended daily intake and eliminates the need for fortification and enrichment. This review provides a general overview of the physical properties and nutritional composition of teff grains related to processing and applications in the food and feed industries. The current status of teff utilization, as well as the challenges in production and commercialization, and future opportunities is presented and discussed.     

Effects of nisin concentration on properties of gelatin film-forming solutions and their films

The addition of nisin into a gelatin matrix can change properties of the film. The aim of this work was to develop gelatin-based films containing different nisin concentrations in order to study their influence on the film's antimicrobial and physical properties and their rheological properties as a film-forming solution (FFS). The FFS was characterised by rheological assays, and the gelatin-based active films were characterised and assessed by the effects of nisin concentrations on their various properties, including antimicrobial activity. Nisin's concentration affected not only its viscoelastic properties of FFS but also its film solubility in water, film surface roughness and light barrier. The addition of nisin also slightly modified the water contact angle and the mechanical properties of the gelatin films. Finally, the films demonstrated activity against Staphylococcus aureus and Listeria monocytogenes at concentrations above 56 mg of nisin g⁻¹ of gelatin.     

压缩合成食品对人体运动能力的影响

研究选取12名生理指标相对类似的试验对象,通过采用自身对照和交叉平衡的试验设计方法,针对普通膳食和以90军用干粮为例的压缩合成食品对人体运动能力的影响进行了分析,通过测定试验对象进食2组不同营养组成的食品进行运动或训练后、恢复体内的血糖浓度水平、血乳酸浓度、血乳酸清除率、心率变化、相关激素水平变化以及不同氧化变化情况评价普通膳食和压缩合成食品对人体运动能力的影响。试验结果显示,相比于普通膳食,压缩合成食品在高强度运动以及力竭运动后维持人体运动能力方面以及体能恢复方面具有明显优越性。